G3 two pressure low humidity generator installed

It’s been exciting to integrate our brand-new RH Systems G3 two pressure low humidity generator into our lab here in Brighton.  It expands our dew-frost point-moisture capability and enables us to substantially increase our throughput to meet the increased demand for moisture analyser testing and ISO17025 accredited calibration services.

Vacuum isolated condensing saturator eliminates water diffusion

The G3 is a patented low humidity generator based on a vacuum isolated condensing saturator.  The vacuum has two key functions; to thermally isolate the saturator to prevent condensation on components that are cooled to cryogenic temperatures, and to eliminate water diffusion into the system that typically result in errors in the generated moisture value.

Moisture as low as 1 ppb

The G3 can generate -120 °C frost point, (-124 °C dew point) and moisture as low as 1 ppb (0.0001 part per million) effectively enabling us to calibrate any moisture analyser – particularly those deployed in hyper-sensitive environments like semiconductor manufacturing and speciality gases.

One of only two G3’s deployed in Europe

This is one of only two G3’s deployed in Europe so far, and is part of Qrometric’s continued commitment to delivering the highest possible calibration and measurement capabilities.

Technical Director, Ned Hawes, seen below with the G3, says: “The G3 will gives us faster, simultaneous calibration of multiple instruments, and is the perfect laboratory-based complement to our FPG onsite capabilities. From an R&D perspective, it will enable us to thoroughly assess instruments from new suppliers, before we support them in the global market.”

What’s the Cost of Inaccurate Humidity Measurement?

During recent projects with a leading compressed air product and solution manufacturers, an interesting query was posed: what effect would inaccurate humidity-moisture measurement have on energy consumption and cost? A calculation taking into account pressure dewpoint, flow, running hours per year, dryer load, and energy unit cost provided an interesting insight.

Inaccurate measurement in compressed air

Compressed air systems are measured and controlled with dew-point sensors. ISO 8573 is the compressed air standard which defines dew point and other limits; Class 1 specifies a maximum of -70 °C dew point (< 3 ppmV H2O at atmospheric pressure).

At -70 °C dew point, the calculation* identified that a 5 °C dew point inaccuracy would cost €5228 per year for a single dry compressed air system. Multiply that by the many compressed air systems on-site and throughout industry, and that can become a significant waste of money and resources.

Compromised Quality and Yield could be even more costly in other industries

In many other applications, inaccurate humidity-moisture measurement can directly affect the bottom line.

For example, in semiconductor production, the tiniest moisture ingress can contribute to defects, reliability issues, yield loss, and a lower-grade product. If humidity-moisture sensors are inaccurate or drying systems fail in wafer fabrication facilities, manufacturers may experience increased defect rates, yield losses, and reduced production efficiency.

In battery manufacturing, moisture contamination can cause cell failure and thermal runaway, leading to safety incidents in electric vehicles, bicycles and manufacturing plants.

If failures are not catastrophic and do not affect safety or the product directly, inefficiencies can go unnoticed and subprocesses remain suboptimal.

So, the cost of inaccurate humidity measurements can lead to direct and indirect costs that can be substantial.

Batteries in compact housing
Accurate moisture detection in battery production is essential to product integrity

Reducing the risk – finding an alternative strategy

Numerous industrial processes use humidity-moisture sensors to monitor and control water content; to maintain that measurement performance, calibration is generally carried out on a regular schedule. 

Calibration frequency depends on the type of instrument and the criticality of the measurement, but is typically six or 12 months.  This usually requires the sensor to be uninstalled and sent back to the supplier or manufacturer.  So, engineering, change control, and logistics costs can be significant.

This strategy also requires process plants to hold stocks of spare sensors to provide measurement continuity while sensors are away being calibrated, further escalating costs.

It’s no surprise that many users are looking for alternative strategies to maintain or improve measurement performance and save costs.

Moving towards onsite calibration

Qrometric’s FPG Dew-Frost point calibrator is a breakthrough solution that enables manufacturers and process plants to calibrate sensors on-site.

The FPG’s portable benchtop design enables on-site use in production lines, factory environments, workshops, and laboratories. It generates a stable frost point by recirculating the sample gas through a temperature-controlled saturator until thermodynamic equilibrium is reached. Under these conditions, the frost point is defined by the saturator temperature, providing a stable reference for sensor calibration and validation. The FPG can be used as a standalone calibration system or in combination with a transfer standard for enhanced confidence/lower uncertainties.

On-site calibration means that instead of sending hundreds of sensors away each year for calibration, only those that need repair or readjustment need be returned. This advantage removes many hours of downtime, reduces the required backup sensor stock levels, and enables significant cost savings related to the consequences of inaccurate sensors.

A recent cost benefit analysis at a battery production site with fifty dew point sensors concluded that the FPG return on investment was little over a year based only on the cost to calibrate the sensors.

* Example based on:

300 L/s compressor, PSA dryer type  
Running hours per year: 5500
Energy cost: 0.2 €/kWh
Load of the machine: 100% PSA dryer, -70 °C PDP1

 

 

UKAS confirms highest standards at Qrometric

Qrometric’s latest Schedule of Accreditation, issued by the United Kingdom Accreditation Service (UKAS), confirms Qrometric’s laboratory is operating to the very highest standards of range and uncertainty in Dew/Frost Point and Relative Humidity calibration.

Exceptional range for humidity/moisture

Qrometric’s accredited Humidity range now extends to -90 ºC frost point, one of just a few laboratories in the UK that can work at this range for both measurement devices and generators.

In Relative Humidity, Qrometric’s CMC has been reduced to as low as 0.12 %rh. This is considered to be one of the lowest uncertainties accredited in the UK and the best uncertainty Qrometric has returned in over three years of UKAS accreditation.

Excellent standards for temperature in air too

The UKAS Schedule also acknowledges exemplary performance of temperature measurement in air, confirming a range of -10 ºC to +85 ºC with an Expanded Measurement Uncertainty of 0.073 ºC.

Callum Morgan, Calibration Laboratory and Quality Manager at Qrometric, pictured above, says this year’s accreditation shows the commitment the company makes to high-end humidity and temperature calibration.

“We work with National Metrology Institutes, Calibration Laboratories, Research and Industrial organisations who depend on best measurement capability for the integrity of their products, processes and services. This accreditation reflects our investment in delivering the very highest quality.”

An investment in the best equipment and the best solutions

What makes it possible to deliver such high standards? Together with a wealth of experience and knowledge in the team, Callum explains that the RH Systems CGS-240 Humidity Generator is at the heart of Qrometric’s laboratory.

The CGS-240 is a fully automated two-pressure two-temperature humidity generator system capable of continuous, high-accuracy humidity generation over a wide range of humidity, temperature, and flow rates.

Six-sided fluid jacket enables lower uncertainties

Callum explains a key feature is the chamber’s six-sided fluid jacket that enables lower uncertainties and a greater temperature range:

“In older technology, the door is typically excluded from the temperature control. In the CGS-240, the temperature-controlled fluid jacket extends across the door, ensuring better thermal gradients and stability. This investment is key to delivering the highest quality for reference labs like us who want to work in the most demanding applications.”

Qrometric’s own FPG Dew Point Calibrator, the world’s first self-contained transportable Dew-Frost Point Calibrator, has also been integral to the laboratory driving for an extended range.

Callum says. “The FPG can operate down to -90, so we need to be able to calibrate our own instrument to that level.”